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By Leonard, John; Lygo, B.; Procter, Garry
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Extra resources for Advanced practical organic chemistry
First of all, carefully review the original objectives of the project and then organize your compound data sheets into a logical order based on how the project progressed with respect to the objectives. This collection of data sheets will eventually become your experimental section. 32 Advanced practical organic chemistry Having reviewed your experimental work, you should have a clear picture of the key achievements made during the course of the project. During many research projects, the original objectives will not have been accomplished, and it may at first seem that much of the work has been unsuccessful.
Consequently, combustion analysis is not always sufficient and alternative purity tests combined with highresolution MS (HRMS) measurements are now often required as proof of purity and molecular formula. Popular modern methods for purity analysis include 1H NMR peak integration relative to an internal standard and HPLC or GC quantification relative to a sample of known purity. The level of detail needed for compound characterization purposes will depend on the structural complexity of the molecule and on where the data will be reported.
Store your chemicals in clearly labeled containers and abide by the regulations concerning storage of solvents and other hazardous materials. Dispose of waste chemicals safely, according to the approved procedures for your laboratory. Never pour organic compounds down the sink. 3 Safety risk assessments Always assess the risks involved before carrying out a reaction. It is good practice to carry out a systematic risk assessment for any new experiment that you intend to carry out, reviewing the hazards associated with the chemicals being used as well as the equipment and experimental procedure.
Advanced practical organic chemistry by Leonard, John; Lygo, B.; Procter, Garry